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; Sieber, S; Schleyer, P v R, J Am Chem Soc, 1996, 118, 3761 3762 81 Maerker, C; Schleyer, P v R; Koch, W; Rauk, A; Sorensen, T S; Mareda, J, J Am Chem Soc, in press 82 (a) Schmidt, H; Schweig, A, Tetrahedron Lett, 1973, 981 (b) Schmidt, H; Schweig, A, Angew Chem Int Ed Engl, 1973, 12, 307 83 (a) Benson, S W, J Chem Ed, 1965, 42, 502 (b) Kerr, J A, Chem Rev, 1966, 66, 465 84 Ho mann, R; Imamura, A; Hehre, W J, J Am Chem Soc, 1968, 90, 1499, and references therein 85 Paulson, B P; Curtiss, L A; Bal, B; Closs, G L; Miller, J R, J Am Chem Soc.

Despite the fact that near infrared spectroscopy (NIR) has been used industrially for decades [36], there has been hesitance to accept and trust new process analytical measurement technologies as equivalent or superior to traditional methods For example, when a discrepancy between online NIR and laboratory analyses is observed, it is rare that the destructive reference methods are ever targeted as the source of error, despite the fact that NIR is often the more precise method The hesitance to trust more advanced, multivariate tools (which are perhaps less directly understood) has certainly been a detriment to progress in deploying PAT Similar concerns persist with regard to chemometrics (multivariate data analysis), information technology (IT), and advanced controls One reason for such behavior may be the practice of calibrating and validating PAT sensors by correlating their signals to traditional, laboratory-based reference methods and characterizing performance in terms of prediction error [37 39].

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802.11- Wireless LAN MAC and PHY Specifications. This is the first 802.11 standard which defines the CSMA/CA MAC scheme and three PHY schemes: Infrared, frequency hopping spread spectrum and direct sequence spread spectrum. 802.11a - Wireless LAN MAC and PHY Specifications: High Speed PHY Layer in the 5 GHz Band. This standard defines the OFDM PHY specification operating at Unlicensed national information infrastructure (UNII) 5 GHz frequency band. 802.11b - Wireless LAN MAC and PHY Specifications: High-speed PHY Layer Extension in the 2.4 GHz Band. This standard is an enhancement of the 802.11 PHY layer in the 2.4 GHz band. It is backward compatible with 802.11. 802.11g - Wireless LAN MAC and PHY Specifications: Further Higher Data Rate Extension in the 2.4 GHz Band. This standard is a further enhancement of 802.11 and 802.11b. It is backward compatible with 802.11 and 802.1lb. 802.11e - This standard has not been finalized yet and is handled by 802.11 Task Group (TG) e. The TG e is working on the enhancement of 802.11 MAC layer to provide better quality of service in 802.11 network. The finalized standard shall be named as 802.11e.

It is a truism of statistics that, no matter how sensitive or accurate the PAT sensor may be in detecting quality variation, the performance of the reference method will always limit the level of perceived accuracy A much more accurate depiction of the performance of PAT sensors compared to reference techniques would be to compare analytical gures of merit, such as signal-to-noise ratio (S/N) or analytical sensitivity, which explicitly account for measurement precision [40, 41] Even though the perceptions of PAT instrumentation have begun to improve, companies continue to worry that the intensity of product quality sampling afforded by PAT sensors will result in negative consequences, such as increased inspection and investigations In other words, many companies continue to fear what they will nd if they begin to analyze their operations more closely.

, 1996, 118, 378 387, and references therein 86 Schleyer, P v R; Kaupp, M; Hampel, F; Bremer, M; Mislow, K, J Am Chem Soc, 1992, 114, 6791 6797 87 Brundle, C R; Robin, M B; Kuebler, N A; Basch, H, J Am Chem Soc, 1972, 94, 1451 88 Kobayashi, T; Miki, S; Yoshida, Z; Asako, Y; Kajimoto, C, J Am Chem Soc, 1988, 110, 5622 89 Honegger, E; Yang, Z Z; Heilbronner, E; Alder, R W; Moss, R E; Sessions, R B, J Elect Spectrosc Rel Phenom, 1985, 36, 297 90 Kimura, K; Katsumata, S; Achiba, Y; Yamazaki, T; Iwata, S, Handbook of He I Photoelectron Spectra of Fundamental Organic Molecules, Halsted, New York, 1981 91 (a) Badger, R M.

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